(Ebook) The Pilot Plant Real Book A Unique Handbook for the Chemical Process Industry 1st Edition by Francis X McConville ISBN 0972176918 9780972176910

(Ebook) The Pilot Plant Real Book A Unique Handbook for the Chemical Process Industry 1st Edition by Francis X McConville ISBN 0972176918 9780972176910

(Ebook) The Pilot Plant Real Book A Unique Handbook for the Chemical Process Industry 1st Edition by Francis X McConville - Ebook PDF Instant Download/Delivery: 0972176918, 9780972176910
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Product details:

ISBN 10: 0972176918 
ISBN 13: 9780972176910
Author: Francis X McConville

(Ebook) The Pilot Plant Real Book A Unique Handbook for the Chemical Process Industry 1st Table of contents:

Chapter 1: The Pilot Plant

• The Role of the Pilot Plant

• Major Factors in Scale-Up

• 12 Things to Do During Process Scale-Up

• 12 Things to Avoid During Process Scale-Up

• Developing Scalable Reactions

• The Role of Calorimetry and Process Safety Screening

• The Haz-Op (Hazard and Operability Study)

• Flow Diagrams and Batch Records

• Good Manufacturing Practices (GMP) in Pilot Plants

Chapter 2: Equipment and Operations

• The Pilot Plant Equipment Train

• Notes on Equipment Selection, Installation, and Maintenance

• Reactors (Types, Selection, Operation)

• Vessel Agitation (Principles, Impeller Types, Scale-Up)

• Charging Raw Materials

• Reaction Control

• Sampling for Reaction Monitoring

• Workup Procedures

• Partition Coefficient and Extraction Efficiency

• Polish Filtration / Decolorization / Water Removal

• Batch Distillation

• Crystallization (Principles, Techniques, Scale-Up)

• Product Isolation

• Filtration Scale-Up

• Product Drying

• Scrubbers

• Reactor and Equipment Cleaning

Chapter 3: Liquid Handling

• Introduction and Terminology

• Pump Sizing and Selection

• Pump Installation and Operation

• Rotary Pump Troubleshooting Guide

• Major Pump Types

• Diaphragm Pump Troubleshooting Guide

• Peristaltic Pump Tubing Sizing and Flowrate Guides

• Pipe, Drawn Tube, and Fittings

• Flanges and Gaskets

• Valves (Types, Selection, Operation)

• Hose and Hose Fittings

• Liquid Velocity and Pressure Effects

• Viscosity Effects

• Standard O-Ring Size Chart

• Rubber Stopper Sizes

• Ground Glass Joint Sizes

• Capacity of Liquid Storage Tanks

• Storage Drum and Shuttle Data

Chapter 4: Heat Transfer

• Heat Transfer in Stirred Tank Reactors

• Typical Batch Cooling Profiles

• Reactor Heat Transfer Coefficients

• Experimental Determination of Heat Transfer Coefficient

• Heat Exchanger Fundamentals

• Example Heat Exchanger Problem

• Chart for Estimating Log Mean Temperature Difference

• Temperature Control Units (TCUs)

• System Start-up and Operation

• Tips on Using Heat Transfer Fluids in TCUs

• Heat Transfer Fluid Selection

• Specific Heat of Various Heat Transfer Fluids vs. Temperature

• Useful Temperature Ranges and Properties of Commercial HTFs

• Notes on the Use of Glycol HTFs

• Specific Gravity of Aqueous Glycol Solutions

• Freezing Points of Aqueous Glycol Solutions

• Boiling Points of Aqueous Glycol Solutions

• Specific Heats of Aqueous Glycol Solutions

• Viscosity of Aqueous Ethylene Glycol Solutions

• Freezing Points of Brines

• Steam Pressure vs. Temperature

• Notes on Process Chillers

• Approximate Chiller Capacity

• Effect of Condenser Cooling Water Temperature

Chapter 5: Electricity and Instrumentation

• Notes on Electrical Safety

   

• Electric Power Basics

   

• Wire Data

   

• Standard Resistor Color Code

   

• Tips on Making Electrical Connections

   

• Receptacle Data

   

• Electrical Enclosure Data

   

• Hazardous Location Classifications for Electrical Equipment

   

• Intrinsically Safe Equipment

   

• Electric Motors (Types, Selection, Troubleshooting)

   

• Motor Nameplate Data

• Typical Current Draw of Induction Motors

• Common Types of Motor Enclosures

• Electric Motor Troubleshooting Guide

• Standard NEMA Motor Frame Sizes

• Temperature Measurement (Thermocouples, RTDs)

• The 4-20 mA Transmitter

• Pressure Measurement

• Flow Measurement

• Level Measurement

• pH Measurement and Control

• Notes on Process Control

• Analog vs. Digital Control Networks

• Understanding PID Controllers

Chapter 6: Solvents

• Safe Handling of Solvents

• Properties and Selection of Solvents

• Solubility Map

• Temperature/Vapor Pressure Relationships

• Distillation Characteristics of Solvents

• Binary Azeotropes

• Ternary Water-Containing Azeotropes

• Water Data (Properties and Usage)

Chapter 7: Compressed Gases

• Safe Handling of Compressed Gases

• Physical Properties of Common Gases

• Cryogenic Liquids

• Cylinder Specifications and Conversion Chart

• Connection Data (Regulators, Fittings)

• Pressure Regulators

• Gas Metering

• Air Data (Properties, Dry Air, Humid Air)

• Air Compressors

• Vacuum Systems

Chapter 8: Chemical Data

• Properties of Acids and Bases

• Dilutions (Formulas and Examples)

• pKa Values

• pH Buffers

• Color Indicators

• Aqueous Solubility Data

• Aqueous Solution Density

• Organic Functional Groups

• Common Reaction Types (Overview for Process Development)

Chapter 9: Chemical Hygiene and Safety

• Safe Handling of Chemicals

• Material Safety Data Sheets (MSDSs) / Safety Data Sheets (SDSs)

• Hazards Classifications

• Labeling Requirements

• Fire Safety (Classes of Fire, Extinguishers)

• Personal Protective Equipment (PPE) Selection

• Glove Selection Guide (Chemical Compatibility)

• Respirators

• Incompatible Chemicals

Chapter 10: Materials Selection

• Properties of Elastomers

• Properties of Plastics

• Properties of Metals

• Properties of Glass

• Metallic Corrosion Data

• Glass Corrosion

• Material Compatibility Table (for various chemicals)

Chapter 11: Miscellaneous

• (This chapter often contains various useful charts, tables, formulas, and practical tips that don't fit neatly into other categories, such as unit conversions, general engineering formulas, project management tips for pilot plants, etc.)

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