(Ebook) Pharmaceutical Process Scale Up 2nd edition by Michael Levin 1574448765 9781574448764

(Ebook) Pharmaceutical Process Scale Up 2nd edition by Michael Levin 1574448765 9781574448764

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ISBN-10 :  1574448765 

ISBN-13 :  9781574448764

Author:  Michael Levin 

With step-by-step methods of drug production and knowledge of major unit operations and key concepts of pharmaceutical engineering, this guide will help to improve communication among the varied professionals working in the pharmaceutical industry. Key features: REVISION OF A BESTSELLER - Updates include recent advances in the field to keep pharmac

Pharmaceutical Process Scale-Up 2nd Table of contents:

1. Introduction
Part I. Fundamentals
2. Fluid Flow
Introduction
Viscosity
Compressibility
Surface Tension
Fluids At Rest: Hydrostatics
The Measure of Pressure Intensity
Fluids in Motion
Bernoulli’S Theorem
Flow Measurement
Laminar and Turbulent Flows
Liquid Flow in Pipes
Streamline Flow in a Tube
Dimensional Analysis and Flow Through a Tube: A General Approach
The Significance of Reynolds Number, Re
Calculation of the Pressure Drop in A Pipe Due To Friction
Flow in Tubes in Noncircular Cross Section
Frictional Losses At Pipe Fittings
Motion of Bodies in A Fluid
Flow of Fluids Through Packed Beds
Pumps
Positive Displacement Pumps
Centrifugal Impeller Pumps
Other Impeller Pumps
3. Heat Transfer
Introduction
The Transfer of Heat Between Fluids
Heat Transfer Through A Wall
Heat Transfer in Pipes and Tubes
Heat Exchange Between A Fluid and A Solid Boundary
Application of Dimensional Analysis To Convective Heat Transfer
Heat Transfer To Boiling Liquids
Pool Boiling
Boiling Inside A Vertical Tube
Boiling with Forced Circulation
Heat Transfer From Condensing Vapors
Dropwise Condensation
Condensation of A Pure Vapor
Condensation of Mixed Vapors
Heat Transfer By Radiation
Exchange of Radiation
Example Problems
4. Mass Transfer
Introduction
Molecular Diffusion in Gases
Equimolecular Counterdiffusion
Diffusion Through A Stationary, Nondiffusing Gas
Molecular Diffusion in Liquids
Mass Transfer in Turbulent and Laminar Flow
Interfacial Mass Transfer
5. Powders
Introduction
Particle Properties
Origins
Structure
Properties
Particle Interactions
Measurement of the Effects of Cohesion and Adhesion
Flow of Powders
Packing of Powders
Granulation
Fluidization
Mixing and Blending
Conclusion
Part II. Processes
6. Air Conditioning and Humidification
Introduction
Vapor and Gas Mixtures
Hygrometry, the Measurement of Humidity
Humidification and Dehumidification
7. Drying
Introduction
The Theory of Drying
Evaporation of Water Into An Airstream
Static Beds of Nonporous Solids
The Internal Mechanism of Drying
Static Beds of Porous Solids
Through-Circulation Drying
Methods Involving Movement of the Solid
Other Methods of Drying
Solids Moving Over A Hot Surface
Batch Dryers
Hot Air Ovens
Vacuum Tray Dryers
Tumbling Dryers
Fluidized Bed Dryers
Agitated Batch Dryers
Freeze-Drying
Continuous Dryers
Spray Dryers
Drum Dryers
8. Solid-Liquid Extraction
Introduction
Methods of Leaching
Leaching By Percolation
Leaching By Immersion
The Choice of Extraction Method
The Choice of Solvent
Factors Affecting the Rate of Leaching
The Size and Size Distribution of the Solid Particles
Temperature
The Physical Properties of the Solvent
The Relative Movement Imposed on the Solids and the Liquid
9. Crystallization
Introduction
Crystallization in Melts
Nucleation
Crystal Growth
Crystallization From Solutions
Principles Underlying the Design and Operation of Crystallizers
Production of Very Fine Crystals
Production of Large Crystals
Crystallizers
Cooling Crystallizers
Evaporative Crystallizers
Vacuum Crystallizers
10. Evaporation and Distillation
Evaporation
Heat Transfer to Boiling Liquids in an Evaporator
The Physical Properties of Solution and Liquids
The Relation Between Boiling Temperature and Solute Concentration
The Relation of Boiling Temperature and External Pressure
The Relation of Viscosity with Temperature and Solute Concentration
The Effect of Temperature on Solubility
The Effect of Heat on the Active Constituents of a Solution
Evaporators
Natural Circulation Evaporators
Forced Circulation Evaporators
Film Evaporators
The Efficiency of Evaporators
Vapor Removal and Liquid Entrainment
Evaporation without Boiling
Distillation
Binary Mixtures of Immiscible Liquids: Steam Distillation
Binary Mixtures of Miscible Liquids
The Relation of Vapor Pressure and Mixture Composition
The Relation of Boiling Point and Mixture Composition
Vapor-Liquid Equilibrium Diagrams
Simple or Differential Distillation
Rectification or Fractionation
Plate Columns
The Principles of Continuous and Batch Fractionation
Separation of Azeotropes and Liquids of Similar Volatility
Molecular Distillation
11. Filtration
Introduction
Clarification
Cake Filtration
The Theories of Filtration
Flow of Fluids Through Porous Media
Factors Affecting the Rate of Filtration
Pressure
Viscosity
Filter Area
Permeability Coefficient
The Retention of Particles in a Depth Filter
The Conditioning of Slurries
The Compressibility of Cakes
Cake Washing and Dewatering
Filters
Gravity Filters
Vacuum Filters
Pressure Filters
Filter Media
Rigid Media
Flexible Media
The Filtration of Air
The Mechanism of Air Filtration
The Design, Operation, and Testing of Air Filters
The Centrifuge
Centrifugal Filtration
Centrifugal Sedimentation
12. Size, Reduction and Classification
The Importance of Fine Particles in Pharmacy
Fundamental Aspects of Crushing and Grinding
The Efficiency of Grinding
The Operation of Mills
Dry and Wet Grinding
Contamination
Temperature Sensitivity
Structural Changes
Dust Hazards
Grinding Equipment
Edge and End Runner Mills
Hammer Mill
Pin Mill
Ball Mill
Vibratory Mill
Fluid Energy Mill
Colloid Mills
Roller Mills
Classification Or Size Separation
Sieving and Screening
Elutriation and Sedimentation
13. Mixing
Introduction
The Scale of Scrutiny
The Mixing of Solids
Some Properties of a Random Mixture
The Degree of Mixing
The Mechanism of Mixing and Demixing
The Rate of Mixing
Mixing Machines
Trough, Ribbon, and Paddle Mixers
Tumbler Mixers
Mullers and Impact Millers
The Mixing of Liquids
Paddle Mixers
Propeller Mixers
Turbines
The Mixing of Liquids and Solids
14. Solid Dosage Forms
Introduction
Granulation
Hard Capsules
Tablets
Inhalation Products
15. Sterilization
Introduction
Thermal Stabilization
Dry Heat
Moist Heat
Radiation
Resistance to Damage
Product Development
Ethylene Oxide
Sterile Filtration
Adsorption and Screening
Filter Integrity
Product Development Considerations
16. Bioprocessing
Introduction
Pharmaceutical Water Systems
Pretreatment and Sources of Water
Water for Injection
Ion Exchange
Distillation
Reverse Osmosis
Storage and Distribution
Quality Control
Validation
Cell Kinetics
Definitions
Growth Cycle
Monod Kinetic Parameters
Bioreactor Design
Background
Rheology
Mass Transfer
Mixing
Heat Transfer
Shear
Bioprocessing Plant Design
Protein Purification
Part III. Quality Principles
17. Quality by Design
Introduction
Regulatory Initiative
Tools for Process Development
18. Statistical Experimental Design
Introduction
Sampling
Randomized and Latin Square Designs
Factorial Design
Fractional Factorial Design
Central Composite Design
Response Surface Maps
Design Space
19. Process Analytical Technology
20. Conclusion
References
Bibliography

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