(Ebook) Methods of Soil Analysis Part 3 Chemical Methods 1st Edition by DL Sparks, AL Page, PA Helmke, Richard H Loeppert ISBN 9780891188254 0891188258

(Ebook) Methods of Soil Analysis Part 3 Chemical Methods 1st Edition by DL Sparks, AL Page, PA Helmke, Richard H Loeppert ISBN 9780891188254 0891188258

(Ebook) Methods of Soil Analysis Part 3 Chemical Methods 1st Edition by DL Sparks, AL Page, PA Helmke, Richard H Loeppert - Ebook PDF Instant Download/Delivery: 9780891188254 ,0891188258
Full download (Ebook) Methods of Soil Analysis Part 3 Chemical Methods 1st Edition after payment

Product details:

ISBN 10: 0891188258
ISBN 13: 9780891188254
Author: DL Sparks, AL Page, PA Helmke, Richard H Loeppert

(Ebook) Methods of Soil Analysis Part 3 Chemical Methods 1st Edition Table of contents:

1
Chapter 1 Sampling
Introduction
Variation of Soils
Sampling Plans
Judgment Sample
Simple Random Sample
Stratified Random Sample
Systematic Sample
Sources of Errors
Subsampling
Composite Samples
References
2
Chapter 2 Quality Assurance and Quality Control
Scope
Sampling
Physical Testing
Chemical Testing
Policy Statement
Authority
Goal
Responsibility
Definitions
Quality Assurance
Quality Control
Defensibility
Traceability
Quality Assurance Manual
Standard Operating Procedures
Organization
Analytical Methods
Record Keeping
Training
Facilities
Instruments and Equipment
Data Management
Documentation
Assessment
Internal
External
Proficiency Testing
Quality Control
Definitions
Test Portion
Replicate
Duplicates
Spiked (or Fortified) Samples
Quality Control Check Samples
Laboratory Control Samples
Standard Reference Materials
Control Charts
Precision
Reproducibility
Accuracy
Bias
Statistical Process Control
Statistics
Control Charts
Outliers
Precision
Precision of the Analysis
Evaluating Sources of Imprecision
Repeatability and Reproducibility
Accuracy
True Value
Bias
Contamination
Blind Duplicates and Split Samples
Scenario One
Scenario Two
Calibration
Range of Analysis
Method Detection Limit
Limit of Quantitation
Limit of Linearity
Linear versus Quadratic Calibration Curves
References
3
Chapter 3 Dissolution for Total Elemental Analysis
Sources of Error in Dissolution of Solids
Principles
Digestion with Aqua Regia and Hydrofluoric Acid
Digestion with Hydrofluoric, Perchloric and Sulfuric Acids
Fusion with Alkali Carbonate
Fusion with Sodium Peroxide
Microwave Digestion
Safety Notes
Method for Preparation of Samples
Special Apparatus
Procedure
Comments
Method for Digestion with Aqua Regia and Hydrofluoric Acid in a Closed Vessel
Special Apparatus
Reagents
Procedure
Comments
Method for Digestion with Hydrofluoric, Sulfuric, and Perchloric Acids
Special Apparatus
Reagents
Procedure
Comments
Method for Pretreatment of Soils High in Ferric Oxide and Manganese Dioxide
Special Apparatus
Reagents
Procedure
Method for Fusion with Sodium Carbonate
Special Apparatus
Reagents
Procedure
Comments
Method for Sodium Peroxide Fusion
Special Apparatus
Reagents
Procedure
Comments
Method for Decomposition with Microwave Digestion
Special Apparatus
Reagents
Procedure
Comments
References
4
Chapter 4 Atomic Absorption and Flame Emission Spectrometry
Principles
Comparison of Techniques
Instrumentation
Light Sources
Atomization Systems
Optical System
Sensitivity and Detection Limits
Interferences
Nonspectral Interferences
Spectral Interferences
Sample Preparation
Soil Digests
Soil Solutions and Soil Extracts
Specialized Sample Introduction Methods
Hydride Generation
Cold Vapor Method
Solid Samples
Flow Injection
References
5
Chapter 5 Inductively Coupled Plasma Emission Spectrometry and Inductively Coupled Plasma-Mass Spectrometry
Inductively Coupled Plasma-Atomic Emission Spectrometry and Inductively Coupled Plasma-Mass Spectrometry
Instrumentation
Analytical Capabilities
Practical Applications
Quality Control Methods
Summary
References
6
Chapter 6 Neutron Activation Analysis
Principles
Neutron Induced Reactions
Neutron Capture Cross-Sections
Production and Decay of Radioactive Isotopes
Nuclear Decay and Detection of Radiation
Equipment
Neutron Sources
Gamma-Ray Detectors
Multichannel Analyzers
General Methods
Radiation Safety
Preparation of Samples for Neutron Irradiation
Neutron Irradiation
Radioassay
References
7
Chapter 7 Elemental Analysis by X-Ray Fluorescence Spectroscopy
Principles
Nature and Production of X-Ray Spectra
Interaction of X-Rays with Matter
Instrumentation
Wavelength-Dispersive Spectrometers
Energy Dispersive Spectrometers
Advantages/Disadvantages of Wavelength-Dispersive Spectrometers and Energy-Dispersive Spectrometers
Equipment Selection and Safety
Analytical Capabilities
Qualitative Analysis
Quantitative Analysis
Sample Preparation Techniques
Loose Powders
Pressed Pellets
Fused Discs
Thin Films
Liquid Samples
Methods for Analysis of Major Elements
Preparation of Glass Discs
Analysis of Minor and Trace Elements in Soil and Plant Samples
Preparation of Pressed Powder Pellets
Elemental Analysis of Loose Powder and Liquid Samples
Other Applications
References
8
Chapter 8 Liquid Chromatography
Principles
High-Performance Liquid Chromatography
Instrumentation
Columns
Separation Methods
Eluents (Mobile Phases)
Detectors
Recorders
Applications
Comments
Ion Chromatography
Instrumentation
Eluent-Suppressed System
Eluent-Nonsuppressed System
Columns
Separation Methods
Eluents
Detectors
Recorders
Applications
References
9
Chapter 9 Differential Pulse Voltammetry
Direct Current and Normal Pulse Polarography
Direct Current Polarography
Normal Pulse Polarography
Differential Pulse Polarography
Principles
Applications
Anodic Stripping Voltammetry
Principles
Applications
Modem Voltammetric Techniques
Instruments and Electrodes
Instruments
Indicator Electrodes
General Methods
Application to Soil Solutions and Natural Waters
Complexation and Speciation
Oxidation-Reduction
Chemical Analysis
Interferences and Other Problems
Conclusions
Acknowledgments
References
10
Chapter 10 Fourier Transform Infrared and Raman Spectroscopy
Theory
Molecular Energy
Molecular Vibrations
Infrared Absorption
Raman Scattering
Vibrational Analysis
Fourier Transform Infrared Spectrometers
Principles of Operation
Data Collection
Spectral Processing Considerations
Spectral Analysis
Comparison to Raman Spectroscopy
Sampling Methods
Transmission Methods
Self-Supporting Films
Diffuse Reflectance
Attenuated Total Reflectance
Fourier Transform Infrared Microspectroscopy
Low Temperature Studies
Raman Microprobe
Acknowledgments
References
11
Chapter 11 Electron Spin (or Paramagnetic) Resonance Spectroscopy
Theory and Principles
The Resonance Phenomenon
Spectral Parameters
The g-Factor
The ESR Experiment
Instrumentation
Sample Preparation
Precautions, Sensitivity, Resolution
Physico-Mathematical Determination and Theoretical Interpretation of Spectral Parameters
Applications to Soil Systems
Whole Soil
Organic Paramagnetic Species in Soil
Interpretation, Examples, and Comments on Electron Spin Resonance Data
Paramagnetic Transition Metal Ion Complexes with Soil Organic and Mineral Materials
Spin Derivatization in Soil Chemistry
Electron Spin Resonance-Related Spectroscopies
Electron Nuclear Double Resonance Spectroscopy
Electron Spin Echo Spectroscopy
Comments
References
12
Chapter 12 X-Ray Photoelectron Spectroscopy
X-Ray Photoelectron Spectroscopy Principles
X-Ray Photoelectron Spectroscopy Instrumentation
Referencing Binding Energy
X-Ray Photoelectron Spectroscopy Analysis
Spin Orbit Splitting
Satellites
Multiplet Splitting
Atomic Concentrations Calculations
Angle Resolved X-Ray Photoelectron Spectroscopy and Depth Profile Studies
Sample Preparation
Sampling Handling and Treatment
Recent Advances and Developments
Acknowledgments
References
13
Chapter 13 X-Ray Absorption Fine Structure Spectroscopy
Physical Basis of X-Ray Absorption Fine Structure
Synchrotrons and Beam Line Hardware
Experimental and Data Analysis
Extended X-Ray Absorption Fine Structure Analysis of Soil Materials
Data Analysis Programs
Sources of Further Information
References
14
Chapter 14 Salinity: Electrical Conductivity and Total Dissolved Solids
Introduction
Saturation and other Aqueous Extracts
Principles
Apparatus
Reagent
Procedure
Calculations
Comments
Electrical Conductivity of Waters and Aqueous Extracts
Principles
Apparatus
Reagents
Procedure
Calculation
Comments
Electrical Conductivity of Saturated Soil Pastes and Determination of Soil Salinity
Principles
Apparatus
Reagents
Procedure
Calculation
Comments
Total Dissolved Solids in Waters and Aqueous Extracts
Principles
Apparatus
Procedure
Calculation
Comments
References
15
Chapter 15 Carbonate and Gypsum
Carbonate
Total Carbonate Analysis
Pressure Calcimeter Method
Gravimetric Method
Simple Titrimetric Procedure
Volumetric Calcimeter Method
Gravimetric Method for Loss of Carbon Dioxide
Acetic Acid Dissolution Method
Carbonate Reactivity
Carbonate Reactivity by pH Stat
Carbonate Reactivity by a Manometric Procedure
Active Carbonate
Carbonate Equilibria-Solid Phase
Principles
Reaction Rates
Extraction of Soil Water for Carbonate Equilibrium Determinations
Gypsum
Method
References
16
Chapter 16 Soil pH and Soil Acidity
Definition of pH
Significance of Soil pH Values
Presence of Free Acids
Presence of Aluminum Ions
Presence of Hydroxy-Aluminum
Presence of Calcium Carbonate
Presence of Sodium Carbonate
Factors Which Affect Soil pH
The Effect of Dilution
Salt Content
Carbon Dioxide Content
Suspension Effect
Fundamentals of pH Measurement
Colorimetric Determinations of pH
Electrometric Measurements
Electrometric Measurement of Soil pH
Equipment
Standardization of the Meter
Electrode Problems
Procedure for Soil pH Measurement
Equipment and Reagents
Determination-pH in Water
pH in One-One Hundredth Molar Calcium Chloride
pH in One Molar Potassium Chloride
Alternative Methods for pH Measurement
Use of Microelectrodes
Use of Test Kits
pH Papers
References
17
Chapter 17 Lime Requirement
Introduction: Definition and Importance of Lime Requirement Methods
Factors Affecting Lime Requirement
Nature of Soil Acidity
Neutralization Sequence: Initial and Desired pH
Soil Properties
Analytical Considerations
Lime Requirement Methods
Field Estimation of Lime Requirement
Soil-Lime Incubations
Soil-Base Titrations
Soil-Buffer Equilibrations
Exchangeable Aluminum
Other Lime Requirement Methods
References
18
Chapter 18 Aluminum
Total Aluminum
Introduction
Principles
Fusion and Dissolution Methods for Total Aluminum
Comments
Alternative Procedure for Total Aluminum
Exchangeable and Extractable Aluminum
Extraction from Mineral Soils with Unbuffered Salts
Extraction of Aluminum from Organic Matter and Organic Soils
Extraction of Aluminum from Poorly Ordered Phases
Sampling Aluminum in Soil Solutions
Introduction
In Situ Sampling with Lysimeters
Extraction of Soil Samples in the Laboratory
Filtration of Soil Solution Samples
Chemical Speciation of Solution Aluminum
Introduction
Timed Spectrophotometric Assays
Physicochemical Separation Methods
Spectrophotometric Methods for Aluminum Analysis
Introduction
8-Hydroxyquinoline-Butyl Acetate
Alternate Spectrophotometric Methods
Atomic Absorption and Inductively Coupled Plasma Optical Emission Spectrometry
Atomic Absorption and Atomic Emission Spectrometry
Plasma Emission and Plasma Mass Spectrometry
Alternative Methods for Aluminum Analysis
X-Ray Fluorescence Spectrometry
Titrimetric Methods
References
19
Chapter 19 Lithium, Sodium, Potassium, Rubidium, and Cesium
General Introduction
Properties of the Alkali Metals
Mineralogy of Alkali Elements in Soils
Potassium
Sodium
Lithium, Rubidium, and Cesium
Analytical Methods for the Alkali Metals
Analysis for Total Alkali Elements
Hydrofluoric Acid Digestion for Total Alkali Elements
Measurement of Soil Potassium
Exchangeable Potassium
Nonexchangeable Potassium
Mineral Potassium Analyses
Soil Tests for Potassium
Mehlich 1 Extraction
Mehlich 3 Extraction
Ammonium Acetate Extractable Potassium
Morgan Extraction
Modified Morgan Extraction
Ammonium Bicarbonate-Diethylenetriamine Pentaacetic Acid Extraction
Exchangeable and Soluble Sodium
Introduction
Procedure
Lithium, Rubidium, and Cesium
Introduction
Procedure for Extractable Lithium or Rubidium
References
20
Chapter 20 Beryllium, Magnesium, Calcium, Strontium, and Barium
Properties of Alkaline-Earth Metals
Mineralogy and Distribution of Beryllium, Magnesium, Calcium, Strontium, and Barium in Rocks and Soils
Total Elemental Magnesium, Calcium, Strontium, Barium, and Beryllium
Introduction
Digestion Methods
Analysis by Atomic Absorption Spectroscopy
Analysis by Inductively Coupled Plasma-Atomic Emission Spectrometry
X-Ray Fluorescence
Suspended Solids by Inductively Coupled Plasma-Atomic Emission Spectrometry
Ion Beam
Partitioning of Alkaline-Earth Metals in Soils
Introduction
Soluble
Extractable/Exchangeable Fraction
Availability Indices
Analytical Methods
Introduction
Atomic Absorption Spectrophotometry
Inductively Coupled Plasma
Electrothermal Atomic Absorption
Flame Emission Photometry
Ion Chromatography
Titrimetric
Permanganate Method
Colorimetric
References
21
Chapter 21 Boron
Principles and Concepts in Boron Chemistry
Boron Chemistry in Aqueous Media
Boron Adsorption-Desorption by Soil Constituents
Boron Extraction Methods
Total Boron in Soil-Fusion Method
Boron Availability Assessment for Plant Uptake
Boron Determination
Colorimetric Methods
Potentiometric Methods
Inductively Coupled Plasma Spectrometry
References

People also search for (Ebook) Methods of Soil Analysis Part 3 Chemical Methods 1st Edition:

laboratory methods of soil and plant analysis
    
manual on soil sampling and methods of analysis
    
methods of soil analysis soil science society of america
    
nitrogen-total. methods of soil analysis
    
methods of testing soil nutrients

Tags: DL Sparks, AL Page, PA Helmke, Richard H Loeppert, Soil Analysis, Chemical Methods